Determination of terpenoids in wines by solid phase extraction and gas chromatography

نویسندگان

  • Zulema Piñeiro
  • Miguel Palma
  • Carmelo G. Barroso
چکیده

A new method for determination of volatile terpenoids in wine is proposed. An off-line solid phase extraction—gas chromatographic method has been used for the determination. The influence of several extraction variables was studied, including the solid phase employed (C-18 versus divinylbenzene-based), eluting solvent (n-pentane, dichloromethane, ethanol and methanol), volume of eluting solvent (1–4 ml) and drying time (0–20 min). Complete recovery of volatile terpenoids from several kinds of wines was obtained under the optimized conditions. © 2004 Elsevier B.V. All rights reserved.

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تاریخ انتشار 2004